Infrared spectroscopy sample preparation method

In the specific operation of infrared spectroscopy, for solid samples, there are four commonly used sample preparation methods: (1) Tableting method, which is to disperse the fine powder of the solid sample uniformly in the alkali metal halide and compress it into A method of transparent flakes; (2) The powder method is to grind a solid sample into a powder below 2 μm, suspend in a volatile solvent, and then spread this suspended droplet on the KBr film base to form after the solvent evaporates A method of uniform powder thin layer; (3) Thin film method is to dissolve the solid sample in an appropriate solvent, pour the solution on a glass slide or KBr window, and produce a uniform thin film after the solvent volatilizes Methods; (4) The paste method is to disperse or suspend the solid powder in a paste such as paraffin oil, and then sandwich the paste between two windows such as KBr to map its spectrum [1]. One of the most commonly used is the tableting method, but this method often needs to be reworked due to problems such as inappropriate sample concentration or opaque films.

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